有機(jī)化學(xué)實(shí)驗(yàn)(陳彪)(英漢雙語(yǔ)教材)
本書(shū)是編者在總結(jié)多年來(lái)有機(jī)化學(xué)實(shí)驗(yàn)的教學(xué)經(jīng)驗(yàn)及近年來(lái)實(shí)施雙語(yǔ)教學(xué)實(shí)踐的基礎(chǔ)上，參考了國(guó)內(nèi)外出版的同類(lèi)教材，采用英漢兩種語(yǔ)言，編寫(xiě)的與有機(jī)化學(xué)雙語(yǔ)課程配套使用的《有機(jī)化學(xué)實(shí)驗(yàn)》教材。
全書(shū)包括：有機(jī)化學(xué)實(shí)驗(yàn)的一般知識(shí)，有機(jī)化學(xué)實(shí)驗(yàn)的基礎(chǔ)知識(shí)和基本操作，有機(jī)化學(xué)綜合實(shí)驗(yàn)（包括合成及分離提取兩大部分），附錄及參考文獻(xiàn)。
本書(shū)可使學(xué)生在掌握有機(jī)化學(xué)實(shí)驗(yàn)基本原理、基本技能的同時(shí)，提高英語(yǔ)實(shí)際應(yīng)用能力和水平，適用于化學(xué)、醫(yī)學(xué)、藥學(xué)及相關(guān)專(zhuān)業(yè)的學(xué)生使用，也可作為有機(jī)化學(xué)及相關(guān)專(zhuān)業(yè)碩士研究生的實(shí)驗(yàn)參考書(shū)。
Chapter 1Introduction of Experimental
Organic Chemistry1
1?1Basic Rules for the Organic
Chemistry Lab1
1?2Common Lab Equipment and
Apparatus2
1?3General Lab Safety7
1?4Disposal of Lab Waste9
1?5Common Organic Solvents9
1?6Experimental Preview Record and
Laboratory Report13
1?7Chemical Literature14
Reference15
Chapter 2Basic Experimental
Techniques17 Chapter 1Introduction of Experimental
Organic Chemistry1
1?1Basic Rules for the Organic
Chemistry Lab1
1?2Common Lab Equipment and
Apparatus2
1?3General Lab Safety7
1?4Disposal of Lab Waste9
1?5Common Organic Solvents9
1?6Experimental Preview Record and
Laboratory Report13
1?7Chemical Literature14
Reference15
Chapter 2Basic Experimental
Techniques17
2?1Heating and Cooling17
2?2Drying and Drying Agent17
2?3Filtration19
2?4Solvent Extraction and Solution
Washing21
2?5The Purification and Separation of
Liquid Organic Substances24
2?6The Purification and Separation of
Solid Organic Substances32
2?7Chromatographic Techniques38
2?8The Determination of the Physical Constant
of Organic Compound47
Chapter 3Comprehensive Experiment56
Part 1Synthesis56
3?1Synthesis of Cyclohexene56
3?2Synthesis of Ethyl Bromide57
3?3Synthesis of 2?chlorobutane
(sec?butyl chloride)59
3?4Synthesis of diethyl ether61
3?5Synthesis of Phenetole
(ethyl phenolate)62
3?6Synthesis of Benzoic Acid and
Benzyl Alcohol63
3?7Synthesis of Acetophenone65
3?8Synthesis of Benzophenone (Friedel?
Crafts acylation method)67
3?9Synthesis of Cyclohexanone69
3?10Synthesis of Adipic Acid71
3?11Synthesis of Benzoic Acid73
3?12Synthesis of Cinnamic Acid74
3?13Synthesis of Ethyl Acetate76
3?14Synthesis of Isoamyl Acetate
(banana oil)78
3?15Synthesis of Acetylsalicylic
Acid (aspirin)79
3?16Synthesis of Methyl Salicylate
(oil of wintergreen)81
3?17Synthesis of Ethyl Acetoacetate83
3?18Synthesis of Acetanilide84
3?19Synthesis of p?toluidine86
3?20Synthesis of Anthranilic Acid
(2?aminobenzoic acid)88
3?21Synthesis of Phenoxyacetic Acid90
3?22Synthesis of Methyl Orange92
3?23Synthesis of Benzocaine94
3?24Synthesis of N?acetyl?p?toluidine96
3?25Synthesis of Benzoin96
3?26Synthesis of 2?Nitroresorcinol98
3?27Synthesis of Quinoline100
3?28Synthesis of Nikethamide103
3?29The Reduction of Camphor104
3?30Synthesis of 3?(2,5?xylyloxyl)
Propyl Chloride and Monitoration of
Reaction Process106
Part 2Extraction and Separation107
3?31The Recrystallization of Benzoic
Acid107
3?32Extraction and Purification of
Nicotine109
3?33Isolation of Caffeine From
Tea Leave110
3?34Isolation of Effective Components
from the Citrus112
3?35Isolation of Benberine from Coptis
chinensis Franch114
3?36Paper Chromatography of Amino
Acid115
3?37Paper Electrophoresis of Amino
Acid117
3?38Separation of Green Leaf Pigments
by TLC119
Chapter 4Appendix121
4?1Experiments from the Literature121
4?2List of the Elements with Their
Symbols and Atomic Masses123
4?3Main Families of Organic
Compounds126
4?4Boling Point and Density of Some
Common Organic Reagents126
第1章有機(jī)化學(xué)實(shí)驗(yàn)基礎(chǔ)知識(shí)127
1?1有機(jī)化學(xué)實(shí)驗(yàn)的基本規(guī)則127
1?2常用的玻璃儀器和實(shí)驗(yàn)裝置127
1?3有機(jī)化學(xué)實(shí)驗(yàn)的安全知識(shí)129
1?4有機(jī)化學(xué)實(shí)驗(yàn)廢物的處置130
1?5常用有機(jī)溶劑及純化130
1?6實(shí)驗(yàn)預(yù)習(xí)記錄和實(shí)驗(yàn)報(bào)告134
1?7有機(jī)化學(xué)的文獻(xiàn)資料134
第2章有機(jī)化學(xué)實(shí)驗(yàn)基本操作136
2?1加熱和冷卻136
2?2干燥與干燥劑136
2?3過(guò)濾137
2?4萃取和洗滌139
2?5液體有機(jī)化合物的分離與純化142
2?6固體有機(jī)化合物的提純147
2?7色譜法151
2?8有機(jī)化合物物理常數(shù)的測(cè)定156
第3章綜合實(shí)驗(yàn)163
第一部分制備163
3?1環(huán)己烯的制備163
3?2溴乙烷的制備164
3?32?氯丁烷的制備165
3?4乙醚的制備166
3?5苯乙醚的制備167
3?6苯甲醇和苯甲酸的制備168
3?7苯乙酮的制備169
3?8二苯甲酮（�；ǎ┑闹苽�171
3?9環(huán)己酮的制備172
3?10己二酸的制備173
3?11苯甲酸的制備175
3?12肉桂酸的制備176
3?13乙酸乙酯的制備177
3?14乙酸異戊酯的制備（香蕉油）178
3?15乙酰水楊酸的制備（阿司匹林）180
3?16水楊酸甲酯的制備（冬青油）181
3?17乙酰乙酸乙酯的制備182
3?18乙酰苯胺的制備183
3?19對(duì)甲苯胺的合成184
3?20鄰氨基苯甲酸的合成185
3?21苯氧乙酸的制備187
3?22甲基橙的制備189
3?23苯佐卡因的制備190
3?24對(duì)甲基?N?乙酰苯胺的合成192
3?25安息香的合成192
3?262?硝基雷瑣酚的制備194
3?27喹啉的制備195
3?28尼可剎米的制備197
3?29樟腦的還原反應(yīng)199
3?30降血脂藥吉非貝齊中間體3?（2，5?二
甲基苯氧基）?1?氯丙烷的制備200
第二部分提取、分離與鑒定201
3?31苯甲酸的提純201
3?32煙堿的提取與鑒定202
3?33從茶葉中提取咖啡因203
3?34橘皮中有效成分的提取、分離
與鑒定205
3?35黃連中黃連素的提取及鑒定206
3?36紙色譜分離鑒定氨基酸208
3?37紙上電泳分離鑒定氨基酸209
3?38薄層色譜法分離葉綠素210
參考文獻(xiàn)212
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